NMR - From spectra to structures 2ed 2007 - Mitchell & Costisella.pdf - eBooks - Tkanczak

Terence N. Mitchell · Burkhard Costisella

NMR – From Spectra to Structures

Terence N. Mitchell · Burkhard Costisella

NMR – From Spectra

to Structures

An Experimental Approach

Second Revised and Expanded Edition

with 168 Figures

123

Terence N. Mitchell

Universität Dortmund

– Fachbereich Chemie –

44227 Dortmund

Germany

e-mail: terence.mitchell@uni-dortmund.de

Burkhard Costisella

Universität Dortmund

– Fachbereich Chemie –

44227 Dortmund

Germany

e-mail: burkhard.costisella@uni-dortmund.de

Library of Congress Control Number: 2007924904

ISBN 978-3-540-72195-6 Springer Berlin Heidelberg New York

ISBN 978-3-540-40695-2 1st ed. Springer Berlin Heidelberg New York 2004

This work is subject to copyright. All rights are reserved, whether the whole or part of

the material is concerned, speciically the rights of translation, reprinting, reuse of il-

lustrations, recitation, broadcasting, reproduction on microilm or in any other way, and

storage in data banks. Duplication of this publication or parts thereof is permitted only

under the provisions of the German Copyright Law of September 9, 1965, in its current

version, and permissions for use must always be obtained from Springer-Verlag. Viola-

tions are liable for prosecution under the German Copyright Law.

Springer-Verlag is a part of Springer Science+Business Media

springer.com

The use of general descriptive names, registered names, trademarks, etc. in this publi-

cation does not imply, even in the absence of a speciic statement, that such names are

exempt from the relevant protective laws and regulations and therefore free for general

use.

Cover design: WMXDesign GmhH, Heidelberg, Germany

Typesetting and production: LE-T E X Jelonek, Schmidt & Vöckler GbR, Leipzig, Germany

Printed on acid-free paper SPIN 12028634 52/3180 YL 5 4 3 2 1 0

dedicated to Reiner Radeglia

an NMR pioneer in a then divided Germany

Preface to the Second Edition

Our attempt to present NMR spectroscopy to the beginner in a somewhat

different way was well-received, so that we were invited by Springer to make

some additions to the original for a second edition. Naturally we have modi-

ied the text to take account of justiied criticisms of the irst edition. We de-

cided immediately to extend the number and scope of the problems section

comprising Part 2, as we know that this section has been very useful to our

readers. We felt that solid-state NMR is now so important and so relatively

easy to do that it would be well worth giving the reader a brief account of its

advantages and disadvantages. And, having already dealt with four important

nuclei in some detail, we decided to add some basic information on a number

of other spin-½ nuclei which are now often studied.

We thank Prof. Janet Blümel, Texas A&M University, and the Gesellschaft

Deutscher Chemiker for allowing us to reproduce solid state NMR spectra.

In addition we thank Klaus Jurkschat and Bernhard Lippert and their groups

for making available samples of organometallic molecules. Thanks also go to

Andrea Bokelmann and Bernhard Griewel for their valuable technical help.

NMR - From spectra to structures 2ed 2007 - Mitchell & Costisella.pdf

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